Nanospeciation Analysis Using Field Flow Fractionation

  1. Moreno-Martin, Gustavo 1
  2. Sanz-Landaluze, Jon 1
  3. Madrid, Yolanda 1
  1. 1 Universidad Complutense de Madrid; Madrid Spain
Revista:
Encyclopedia of Analytical Chemistry

Año de publicación: 2017

Páginas: 1-24

Tipo: Artículo

DOI: 10.1002/9780470027318.A9395 GOOGLE SCHOLAR lock_openAcceso abierto editor

Resumen

Trace element speciation is currently moving toward nanotechnology field. Nanosized materials such as metallic nanoparticles (MNPs) and metallic oxide nanoparticles (MONPs) are being used in many fields. However, their impact on the environment and human health is still poorly understood. Characterizing metal and metalloids in nanosize form is not an easy task, and it is still at an incipient stage of development. There is a current trend of using multimethod approaches to provide information, especially for nano-objects in complex matrices. Field flow fractionation (FFF) techniques, especially asymmetrical flow-field flow fractionation (AF4), have been shown as a promising approach for size-based elemental speciation. This article provides a detailed description of the application of AF4 to trace element speciation in nanosize form. The description will focus first on the difficulties encountered in MNPs and MONPs determination, especially those factors affecting their stability (sample treatment and interaction with living systems). The second part outlines the application of the AF4 in nanospeciation consisting of a description on the basic principles of the technique and the parameters affecting MNPs and MONPs separation along with different methodologies for their sizing and quantification. The article presents throughout selected examples on the application of AF4 for characterizing nanoparticles.

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